Crucibles serve as containers for samples during thermoanalytical measurements. They guarantee that the sensor is not contaminated by the measurement. The type of crucible used for a measurement can have a large effect on the quality of the results obtained, and in addition, also influences important characteristics of the DSC measuring cell. Considering the relevant factors before the measurement can often help to save time later on when interpreting the curve.
Large volume – increases the sensitivity
Low mass-pushes the resolution to the limit
Purity – no interaction of the sample with the crucible
Material – guarantees high thermal conductivity and form stability
Flatness ensures perfect thermal contact and no artifacts
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